• 专利标题:   Antistatic acrylic resin comprises e.g. methyl methacrylate, n-butyl methacrylate, acrylic acid, butyl acrylate, isooctyl acrylate, isobornyl methacrylate, acrylate, benzoyl peroxide, water, neutralizer, n-butanol, and graphene oxide.
  • 专利号:   CN107987208-A
  • 发明人:   YUAN X, YUAN Z
  • 专利权人:   ANHUI KEBANG RESIN TECHNOLOGY CO LTD
  • 国际专利分类:   C08F220/18, C08F220/14, C08F220/06, C08F220/20, C09D133/10, C09D005/24
  • 专利详细信息:   CN107987208-A 04 May 2018 C08F-220/18 201838 Pages: 8 Chinese
  • 申请详细信息:   CN107987208-A CN11482587 29 Dec 2017
  • 优先权号:   CN11482587

▎ 摘  要

NOVELTY - Antistatic acrylic resin comprises 9-10 pts. wt. methyl methacrylate, 9-10 pts. wt. n-butyl methacrylate, 3-4 pts. wt. acrylic acid, 6-7 pts. wt. butyl acrylate, 6-7 pts. wt. isooctyl acrylate, 12-14 pts. wt. isobornyl methacrylate, 4-6 pts. wt. acrylate, 1-2 pts. wt. benzoyl peroxide, 22-25 pts. wt. water, 3-5 pts. wt. neutralizer, 8-10 pts. wt. n-butanol, 46-50 pts. wt. ammonium polyphosphate, 20-25 pts. wt. tetramethylol methane, 20-25 pts. wt. triallyl cyanurate, and 2-14 pts. wt. graphene oxide. USE - Used as antistatic acrylic resin. ADVANTAGE - The anti-static acrylic resin: has excellent compactness, and low expanded thickness; and improves flame resistance of coatings; and the method is simple, safe, and energy-saving and has wide application range. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for preparing the resin comprising (i) adding n-butanol in a reaction kettle at room temperature, heating to 90-100 degrees C, and stirring uniformly, (ii) adding methyl methacrylate, n-butyl methacrylate, acrylic acid, butyl acrylate, isooctyl acrylate, isobornyl methacrylate, hydroxypropyl acrylate and di-benzene monomer, and graphene oxide, stirring uniformly, (iii) uniform speed dropping methyl methacrylate, n-butyl methacrylate, acrylic acid, butyl acrylate, isooctyl acrylate, isobornyl methacrylate, hydroxypropyl acrylate, and benzoyl peroxide for 2-3 hours. raising temperature to 120-130 degrees C, preserving heat for 3-4 hours, reducing temperature to 70-80 degrees C into water, reducing the temperature to 40-50 degrees C, adding neutralizer, stirring for 40-50 minutes, and (iv) adding ammonium polyphosphate, tetramethylol methane, and triallyl cyanurate, stirring for 30-60 minutes, discharging and packing.