• 专利标题:   Preparing nitrogen-doped graphene material, by dispersing graphene in deionized water, adding aqueous solution of 3,5-diamino-1 H-1,2,4-triazole, heating, grinding into powder, heating tubular furnace and obtaining nitrogen-doped graphene.
  • 专利号:   CN110937597-A
  • 发明人:   ZHU J, WU D, YANG X, LIN R, FANG J
  • 专利权人:   UNIV GUANGDONG PETROCHEM TECHNOLOGY
  • 国际专利分类:   C01B032/194
  • 专利详细信息:   CN110937597-A 31 Mar 2020 C01B-032/194 202032 Pages: 7 Chinese
  • 申请详细信息:   CN110937597-A CN11360952 26 Dec 2019
  • 优先权号:   CN11360952

▎ 摘  要

NOVELTY - Method for preparing nitrogen-doped graphene material based on 3,5-diamino-1 H-1,2,4-triazole, involves dispersing graphene in deionized water, adding an aqueous solution of 3,5-diamino-1 H-1,2,4-triazole, heating at 50-100 degrees C for 30-60 minutes, cooling to 0-4 degrees C to obtain graphene-coated 3,5-diamino-1 H-1,2,4-triazole eutectic, grinding into powder, and heating tubular furnace at 500-800 degrees C for 3-5 hours to obtain a nitrogen-doped graphene material, where the mass ratio of the graphene to 3,5-diamino-1 H-1,2,4-triazole in the aqueous solution of 3,5-diamino-1 H-1,2,4-triazole is 1:(1-10). USE - Method for preparing nitrogen-doped graphene material based on 3,5-diamino-1 H-1,2,4-triazole. ADVANTAGE - The method obtains graphene material with high nitrogen doping content, eliminates the need of adhesives and other additives, and completely maintains the surface properties of 3,5-diamino-1 H-1,2,4-triazole crystals.