• 专利标题:   Preparing monolayer graphene oxide based on blue carbon by graphitizing blue charcoal, pre-oxidizing obtained graphite, intercalating oxidation treatment, and exfoliating graphite oxide in aqueous solution.
  • 专利号:   CN112811416-A
  • 发明人:   GUO S, HUANG Y, ZHANG J, GAO S, ZHONG M, TIAN Y, SHEN W, GAO F, YAN J, LI L, HAO Q
  • 专利权人:   SHAANXI YUNENG GROUP ENERGY CHEM RES, UNIV SHANGHAI JIAOTONG
  • 国际专利分类:   C01B032/198
  • 专利详细信息:   CN112811416-A 18 May 2021 C01B-032/198 202153 Pages: 8 Chinese
  • 申请详细信息:   CN112811416-A CN10072228 20 Jan 2021
  • 优先权号:   CN10072228

▎ 摘  要

NOVELTY - Method for preparing monolayer graphene oxide based on blue carbon, involves graphitizing blue charcoal under high temperature conditions, pre-oxidizing the obtained graphite, intercalating oxidation treatment to obtain graphite oxide, and exfoliating the graphite oxide in an aqueous solution to obtain a monolayer graphene oxide dispersion. USE - The method is useful for preparing monolayer graphene oxide based on blue carbon. ADVANTAGE - The method solves the problem of low yield of the separated single-layer graphene and use of sodium nitrate in the Hummers method caused the production of toxic nitrogen oxides during the reaction, and prepares the monolayer graphene at a rate of 99%.