• 专利标题:   Flexible hydrophobic silica aerogels for water purifying system, comprises deionized water, acidic silica sol, methyltriethoxysilane, graphene solution, cetyltrimethylammonium bromide and trimethylchlorosilane.
  • 专利号:   CN106986605-A
  • 发明人:   ZHAO H, XU Y, XIAO L, CHEN J, WANG M
  • 专利权人:   UNIV JILIN CONSTR
  • 国际专利分类:   C04B028/24, C04B038/00, C04B041/49
  • 专利详细信息:   CN106986605-A 28 Jul 2017 C04B-028/24 201760 Pages: 6 Chinese
  • 申请详细信息:   CN106986605-A CN10168926 21 Mar 2017
  • 优先权号:   CN10168926

▎ 摘  要

NOVELTY - Flexible hydrophobic silica aerogels comprises 30-50 pts. wt. deionized water, 6-10 pts. wt. acidic silica sol, 12-20 pts. wt. methyltriethoxysilane, 3-6 pts. wt. of 15mg/ml graphene solution, 0.3-0.5 pts. wt. cetyltrimethylammonium bromide and 8-15 pts. wt. trimethylchlorosilane. USE - Flexible hydrophobic silica aerogels for water purifying system (claimed). ADVANTAGE - The flexible hydrophobic silica aerogels has a hydrophobic property, low density and low heat conductivity, and produced in simple and cost-effective manner, and suitable for industrial production. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a method for preparing flexible hydrophobic silicone aerogels, which involves: (A) adding deionized water to graphene solution, adding cetyltrimethylammonium bromide, adding acidic silica sol, and adjusting the pH of 3-4; (B) adding methyltriethoxysilane, and heating and stirring at 50 degrees C for 0.5 hours; (C) diluting the ammonia water into the solution, adjusting the pH to 6-7 and placing to obtain gel; (D) adding gel in oven at 50 degrees C for 24 hours and drying at 70 degrees C for 24 hours to obtain hydrophilic silicone airgel; and (E) placing in hydrophilic silicone airgel in a reaction kettle, adding 8-15 pts. wt. trimethylchlorosilane, carrying out gas-solid reaction at 70-90 degrees C for 3-6 hours to obtain final product.