• 专利标题:   Preparing polylactic acid fiber using combined plant comprises taking combined plant, shell powder and graphene, fermentation to obtain fermentation liquid, using lime milk, boiling, cooling, re-crystallizing, filtering and centrifugation.
  • 专利号:   CN106958051-A, CN106958051-B
  • 发明人:   WANG J, LI B, LI Y, GU Y, WANG Y, LI P, FU B, LV J
  • 专利权人:   UNIV YUNNAN AGRIC, UNIV YUNNAN AGRIC
  • 国际专利分类:   C12P007/56, D01F001/10, D01F006/92
  • 专利详细信息:   CN106958051-A 18 Jul 2017 D01F-006/92 201756 Pages: 6 Chinese
  • 申请详细信息:   CN106958051-A CN10324637 10 May 2017
  • 优先权号:   CN10324637

▎ 摘  要

NOVELTY - Preparing polylactic acid fiber using combined plant comprises (A) taking the combined plant, shell powder and graphene, fermentation to obtain fermentation liquid, (B) using lime milk to neutralize slight alkalinity of the fermentation liquid, boiling for sterilizing, cooling, filtering and re-crystallizing, (C) slowly adding acetic acid, stirring, filtering, evaporating and concentrating filter liquid, and (D) centrifugation to obtain lactic acid, and (E) dehydration and cyclization the obtained lactic acid to obtain lactide, taking the obtained lactide to ring-opening polymerization. USE - The method is useful for preparing polylactic acid fiber using combined plant (claimed). ADVANTAGE - The method is environmentally friendly and suitable for textile industry. DETAILED DESCRIPTION - Preparing polylactic acid fiber using combined plant comprises (A) taking the combined plant, shell powder and graphene, under action of bio-catalyst, adding pure lactic acid bacteria for fermentation to obtain fermentation liquid, (B) using lime milk to neutralize slight alkalinity of the fermentation liquid, boiling for sterilizing, cooling, filtering and re-crystallizing by hot water, (C) slowly adding acetic acid, stirring, filtering, evaporating and concentrating filter liquid, and (D) centrifugal processing the concentrated liquid at 3500-4500 revolutions/minute to obtain lactic acid, and (E) dehydration and cyclization the obtained lactic acid to obtain lactide, taking the obtained lactide to ring-opening polymerization.