• 专利标题:   Preparing interface polarization enhanced titanium dioxide/reduced graphene oxide wave absorbing material comprises e.g. dispersing graphene oxide in mixed solution of ethanol and water by ultrasonic treatment, vacuum drying and introducing reducing gas into tube furnace for heat treatment.
  • 专利号:   CN114149786-A
  • 发明人:   ZHANG X
  • 专利权人:   SHAANXI RAILWAY INST
  • 国际专利分类:   C09K003/00
  • 专利详细信息:   CN114149786-A 08 Mar 2022 C09K-003/00 202239 Chinese
  • 申请详细信息:   CN114149786-A CN11495449 08 Dec 2021
  • 优先权号:   CN11495449

▎ 摘  要

NOVELTY - Preparing interface polarization enhanced titanium dioxide/ reduced graphene oxide (RGO) wave absorbing material comprises (1) dispersing graphene oxide (GO) in a mixed solution of ethanol and water by ultrasonic treatment to obtain a graphene oxide (GO) suspension, then adding a mixed solution of tetrabutyl titanate and ethanol, and magnetically stirring to obtain a uniform mixed solution, (2) placing the uniformly mixed solution in a polytetrafluoroethylene-lined autoclave to obtain a solid-phase product at a high temperature, (3) washing the solid-phase product with absolute ethanol and water, and then vacuum drying to obtain the titanium dioxide/ graphene oxide nanocomposite material, and (4) placing the titanium dioxide/ graphene oxide nanocomposite material in a tube furnace, and a introducing reducing gas into the tube furnace for heat treatment. USE - The method is useful for preparing interface polarization enhanced titanium dioxide/reduced graphene oxide wave absorbing material. ADVANTAGE - The method forms a nanometer-thick amorphous interface layer on the surface of the titanium dioxide nanoparticle by heat treatment in a hydrogen atmosphere and forms a nanometer heterogeneous interface; and significantly enhances its dielectric loss performance.