• 专利标题:   Preparation of high-quality graphene involves taking concentrated sulfuric acid and natural graphite, uniformly mixing, adding potassium permanganate, reacting, heating, adding potassium permanganate, reacting, hydrolyzing, and drying.
  • 专利号:   CN104495827-A
  • 发明人:   FEI L, HUANG X, WEN G, ZHONG B
  • 专利权人:   HARBIN INST TECHNOLOGY, WEIHAI YUNSHAN TECHNOLOGY CO LTD
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104495827-A 08 Apr 2015 C01B-031/04 201542 Pages: 18 Chinese
  • 申请详细信息:   CN104495827-A CN10834857 30 Dec 2014
  • 优先权号:   CN10834857

▎ 摘  要

NOVELTY - A high-quality graphene is prepared by oxidized graphite by taking 20-40 mL concentrated sulfuric acid and 1 g natural graphite, uniformly mixing at low temperature, preferably 0-25 degrees C, adding potassium permanganate at mass ratio of 1-6:1, reacting at 0-25 degrees C for 1-6 hours, heating at 30-70 degrees C, adding potassium permanganate, reacting at 30-70 degrees C for 1-8 hours, adding deionized water, hydrolyzing at 80-100 degrees C for 5-4 hours to obtain aqueous graphite oxide solution, washing with water, and drying at high temperature. USE - Method for preparing high-quality graphene (claimed).