• 专利标题:   Preparing high-performance nitrogen-doped graphene, comprises placing graphite powder in liquid helium, adding dispersant and thin-layer graphene, obtaining graphene oxide dispersion liquid, subjecting mixed solution of graphene oxide dispersion and nitrogen source to stirring and heat-treating.
  • 专利号:   CN114804087-A
  • 发明人:   WANG L, YU G
  • 专利权人:   NANTONG PULANGKE GRAPHENE TECHNOLOGY CO
  • 国际专利分类:   C01B032/19, C01B032/194
  • 专利详细信息:   CN114804087-A 29 Jul 2022 C01B-032/19 202299 Chinese
  • 申请详细信息:   CN114804087-A CN10465997 29 Apr 2022
  • 优先权号:   CN10465997

▎ 摘  要

NOVELTY - Preparing high-performance nitrogen-doped graphene, comprises placing graphite powder in liquid helium, and placing at 100℃ until the liquid helium is completely vaporized, repeating at least three times, and using high-temperature helium gas flow to grind and peel off the graphite powder for 1-5 hours to obtain thin-layer graphene, adding dispersant and thin-layer graphene successively into organic solvent, obtaining graphene oxide dispersion liquid, where the mass ratio of thin-layer graphene and dispersant is (0.1-3): 1, subjecting the mixed solution of the graphene oxide dispersion and the nitrogen source to stirring or ultrasonic operation, and heat-treating by adding cyanuric chloride. USE - The method is useful for preparing high-performance nitrogen-doped graphene. ADVANTAGE - The method enables to prepare high performance nitrogen-doped graphite that has high purity and good conductive and heat-conducting performance.