• 专利标题:   Preparing graphene-modified cellulose fiber involves performing acid pre-treatment of fiber, adding sodium hydroxide, hydrogen peroxide solution, hydrogen peroxide stabilizer, magnesium sulfate heptahydrate, and graphene solution, performing microwave radiation to mixed solution, beating, and drying.
  • 专利号:   CN115852676-A
  • 发明人:   CAI H, SHI C, SHI Y, TIAN M, CHEN Y
  • 专利权人:   ANHUI DISHENG WEAVING ARRANGEMENT CO LTD
  • 国际专利分类:   D06M010/00, D06M010/06, D06M101/06, D06M011/38, D06M011/50, D06M011/55, D06M011/56, D06M011/74
  • 专利详细信息:   CN115852676-A 28 Mar 2023 D06M-011/74 202332 Chinese
  • 申请详细信息:   CN115852676-A CN11599601 12 Dec 2022
  • 优先权号:   CN11599601

▎ 摘  要

NOVELTY - Method of preparing graphene-modified cellulose fiber involves: (a) performing acid pre-treatment of fiber, and washing with water until the pH value is 6.5-7.5 to obtain pre-treated fiber; (b) adding sodium hydroxide, hydrogen peroxide solution, hydrogen peroxide solution stabilizer, magnesium sulfate heptahydrate, and graphene solution, and mixing; (c) performing microwave radiation to the mixed solution, where the concentration of alkali-oxygen first-bath solution is 5-8 g/L, and the bath ratio of alkali-oxygen first-bath solution to the pre-treated fiber is 18-25:1; and (d) beating mixed solution, water washing, acid washing, and drying. USE - Method of preparing graphene-modified cellulose fiber.