• 专利标题:   Preparing graphene oxide material with high heat radiation coefficient and electromagnetic shielding, involves performing vacuum freeze drying treatment to slurry, carrying out high temperature graphitization treatment, processing cold pressed graphene sample, preheating, spraying and solidifying.
  • 专利号:   CN113666363-A
  • 发明人:   HE X, PENG Q, HOU J, ZHAO X, XU F, FU H
  • 专利权人:   SHENZHEN XICHUANG TECHNOLOGY CO LTD
  • 国际专利分类:   C01B032/184, C01B032/194, C09D001/00, C09D007/61
  • 专利详细信息:   CN113666363-A 19 Nov 2021 C01B-032/184 202236 Chinese
  • 申请详细信息:   CN113666363-A CN10897805 05 Aug 2021
  • 优先权号:   CN10897805

▎ 摘  要

NOVELTY - Preparing graphene oxide material with high heat radiation coefficient and electromagnetic shielding comprises (i) uniformly stirring the graphene oxide slurry; (ii) performing vacuum freeze drying treatment to the uniformly stirred graphene oxide slurry; (iii) carrying out hydrazine hydrate reduction treatment to the material after vacuum freezing and drying treatment; (iv) carrying out high temperature graphitization treatment to the material after the hydrazine hydrate reduction treatment; (v) carrying out vacuum cold pressing treatment to the sample after high temperature graphitization treatment; (vi) processing the coldpressed graphene sample with a machining center; (vii) grinding the surface of the graphene plate by mechanical flat grinding; (viii) preheating the graphene plate by a heating table; (ix) uniformly spraying the heat radiation coating to the surface of the graphene plate; and (x) solidifying the sprayed graphene plate. USE - The method is useful for preparing graphene oxide material with high heat radiation coefficient and electromagnetic shielding. ADVANTAGE - The method solves the current problem of poor heat radiation effect and electromagnetic shielding effect of composite materials. DETAILED DESCRIPTION - Preparing graphene oxide material with high heat radiation coefficient and high electromagnetic shielding comprises (i) uniformly stirring the graphene oxide slurry; (ii) performing vacuum freeze drying treatment to the uniformly stirred graphene oxide slurry; (iii) carrying out hydrazine hydrate reduction treatment to the material after vacuum freezing and drying treatment; (iv) carrying out high temperature graphitization treatment to the material after the hydrazine hydrate reduction treatment; (v) carrying out vacuum cold pressing treatment to the sample after high temperature graphitization treatment; (vi) processing the coldpressed graphene sample with a machining center; (vii) grinding the surface of the graphene plate by mechanical flat grinding; (viii) preheating the graphene plate by a heating table; (ix) uniformly spraying the heat radiation coating to the surface of the graphene plate, where the heat radiation coating comprises zirconium dioxide, ferric oxide, chromium oxide and graphene powder according to ratio of 2:1:2:5-6; and (x) solidifying the sprayed graphene plate.