• 专利标题:   Method of reducing manganese content in graphene oxide involves adding graphite into mixed solution of sulfuric acid and phosphoric acid, adding potassium permanganate and adding mixed acid, filtering, cooling, and adding graphite.
  • 专利号:   CN103395780-A, CN103395780-B
  • 发明人:   HOU S, LIU T, QU F, SU Y
  • 专利权人:   JINING LEADER NANO TECHNOLOGY CO LTD
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103395780-A 20 Nov 2013 C01B-031/04 201406 Pages: 5 Chinese
  • 申请详细信息:   CN103395780-A CN10359461 19 Aug 2013
  • 优先权号:   CN10359461

▎ 摘  要

NOVELTY - Method of reducing manganese content in graphene oxide involves adding graphite into mixed solution containing concentrated sulfuric acid and phosphoric acid, adding potassium permanganate, reacting at 40-60 degrees C for 9-15 hours, adding mixed acid 1-4 times of ice water, stirring uniformly, filtering the solution, cooling to room temperature, adding graphite 3-5 times of hydrogen peroxide solution, washing using distilled water until pH is 4-6, filtering, and obtaining wet material. USE - Method of reducing manganese content in graphene oxide (claimed). ADVANTAGE - The manganese content in graphene oxide is reduced by simple method by reduced water consumption and uniform grain diameter distribution. The content of manganese in graphene oxide is less than 20 ~g/g.