• 专利标题:   Producing a graphene film on catalyst-free insulating substrate comprises e.g. representing two ends of quartz tube as raw material feeding end and base end, placing an insulating substrate and a raw material, sealing, heating and cooling.
  • 专利号:   CN110510602-A
  • 发明人:   QIU H, WU Y, HU Z
  • 专利权人:   UNIV TIANJIN TECHNOLOGY
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN110510602-A 29 Nov 2019 C01B-032/184 201999 Pages: 8 Chinese
  • 申请详细信息:   CN110510602-A CN10900985 23 Sep 2019
  • 优先权号:   CN10900985

▎ 摘  要

NOVELTY - Producing a graphene film on catalyst-free insulating substrate comprises (i) preparing a quartz tube, respectively representing the two ends of the quartz tube as raw material feeding end and as a base end, placing an insulating substrate in the base end and placing a raw material in the raw material feeding end, evacuating the quartz tube, and sealing the quartz tube so the internal pressure of the quartz tube is 10-4-10-6 Pa, where the raw material is polyethylene or polypropylene; and (ii) simultaneously heating the raw material feeding end at 1000-1150 degrees C and base end at 200-900 degrees C for 0.5-1 hour, and cooling to 20-25 degrees C. USE - The method is useful for producing a graphene film on catalyst-free insulating substrate. ADVANTAGE - The graphene film can cover the insulating substrate to more than 1x 2 cm.