• 专利标题:   Preparation of high oil-absorption graphene composite material useful for processing organic reagent leakage, involves adding polyacrylonitrile nanofiber to water, dispersing graphene oxide in water, adding hydrazine, and drying.
  • 专利号:   CN105251459-A
  • 发明人:   CHEN C, CHEN X, HUANG Y, SUN D, YANG J, ZHANG H, WU Q
  • 专利权人:   UNIV NANJING SCI TECHNOLOGY
  • 国际专利分类:   B01J020/26, B01J020/30, C02F001/28
  • 专利详细信息:   CN105251459-A 20 Jan 2016 B01J-020/26 201644 Pages: 12 English
  • 申请详细信息:   CN105251459-A CN10747321 05 Nov 2015
  • 优先权号:   CN10747321

▎ 摘  要

NOVELTY - The preparation method of high oil-absorption graphene composite material involves adding polyacrylonitrile nanofiber and deionized water to a container, electrostatically spinning the mixture to obtain a mixed liquid and then freeze-drying to obtain a three-dimensional polyacrylonitrile nanofiber foam, dispersing graphene oxide in deionized water and performing Hummers method to obtain a graphene oxide dispersion liquid, soaking the three-dimensional polyacrylonitrile nanofiber foam in graphene oxide dispersion liquid, adding hydrazine to the mixture, and drying. USE - The method is useful for preparation of high oil-absorption graphene composite material, which is useful for processing overflow oil and organic reagent leakage. ADVANTAGE - The method enables simple preparation of graphene composite material with excellent high oil absorption properties. DETAILED DESCRIPTION - The preparation method of high oil-absorption graphene composite material involves adding polyacrylonitrile nanofiber and deionized water to a container, uniformly mixing, electrostatically spinning the mixture to obtain a mixed liquid and then freeze-drying to obtain a three-dimensional polyacrylonitrile nanofiber foam, dispersing graphene oxide in deionized water and then performing Hummers method to obtain a graphene oxide dispersion liquid, soaking the three-dimensional polyacrylonitrile nanofiber foam in graphene oxide dispersion liquid and then freeze-drying under vacuum to obtain a graphene oxide/polyacrylonitrile composite material, adding hydrazine to the composite material and then washing using water and alcohol, and drying.