• 专利标题:   Method for preparation of manganese ferrite-graphene composite material, involves adding graphite oxide 2-pyrrolidone, adding ferric acetylacetonate, manganese acetylacetonate and octadecylamine and adding organic solvent.
  • 专利号:   CN105883929-A
  • 发明人:   MA S, MA T, SUN G, YUAN M
  • 专利权人:   UNIV BEIJING NORMAL SCI PARK CO LTD, UNIV BEIJING NORMAL
  • 国际专利分类:   B82Y030/00, C01G049/00, H05K009/00
  • 专利详细信息:   CN105883929-A 24 Aug 2016 C01G-049/00 201670 Pages: 12 Chinese
  • 申请详细信息:   CN105883929-A CN10266615 26 Apr 2016
  • 优先权号:   CN10266615

▎ 摘  要

NOVELTY - The method for preparation of manganese ferrite-graphene composite material, involves adding graphite oxide 2-pyrrolidone, dispersing, adding ferric acetylacetonate, manganese acetylacetonate and octadecylamine, heating, refluxing, adding organic solvent, stopping the reaction, separating the reaction products and washing and drying the reaction product. The mass ratio of graphite oxide and ferric acetylacetonate is 0.1-0.2. The mass ratio of graphite oxide and manganese acetylacetonate is 0.3-0.45. The mass ratio of graphite oxide and octadecyl amine is 1:80-1:40. USE - Method for preparation of manganese ferrite-graphene composite material (claimed). ADVANTAGE - The method enables preparation of manganese ferrite-graphene composite material with average diameter of 10 nm and excellent absorbing performance. DETAILED DESCRIPTION - Method for preparation of manganese ferrite-graphene composite material, involves adding graphite oxide 2-pyrrolidone, dispersing, adding ferric acetylacetonate, manganese acetylacetonate and octadecylamine, heating at 100-150 degrees C for 20-50 minutes, refluxing for 1-5 hours, adding an organic solvent, stopping the reaction, separating the reaction products and washing and drying the reaction product. The mass ratio of graphite oxide and ferric acetylacetonate is 0.1-0.2. The mass ratio of graphite oxide and manganese acetylacetonate is 0.3-0.45. The mass ratio of graphite oxide and octadecyl amine is 1:80-1:40.