• 专利标题:   Preparation of lithium ion battery cathode material involves dispersing graphene powder in dimethyl formamide solution to obtain graphene oxide dispersion, and adding with cobalt salt and polyvinylpyrrolidone to obtain mixed solution.
  • 专利号:   CN106450236-A, CN106450236-B
  • 发明人:   DING Z, LI B, HE Y, CHU X, KANG F
  • 专利权人:   UNIV TSINGHUA SHENZHEN GRADUATE SCHOOL, UNIV TSINGHUA SHENZHEN GRADUATE SCHOOL
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/58, H01M004/587
  • 专利详细信息:   CN106450236-A 22 Feb 2017 H01M-004/36 201725 Pages: 14 Chinese
  • 申请详细信息:   CN106450236-A CN11117716 07 Dec 2016
  • 优先权号:   CN11117716

▎ 摘  要

NOVELTY - The preparation of lithium ion battery cathode material involves dispersing the appropriate amount of graphene powder in dimethyl formamide solution to obtain graphene oxide dispersion, adding cobalt salt and polyvinylpyrrolidone to dispersion to obtain mixed solution, adding mixed solution into hydrothermal reactor, maintaining filling degree of reactor at 75-80%, closing reactor in explosion-proof oven, raising temperature from room temperature to 195-220 degrees C at rate of 3-5 degrees C/minute for 20-40 hours, natural cooling to collect the precipitate in reactor, washing, and drying. USE - Preparation of lithium ion battery cathode material (claimed). ADVANTAGE - The method enables preparation of lithium ion battery cathode material with stable small rate cycle performance by simple and controllable process. DETAILED DESCRIPTION - The preparation of lithium ion battery cathode material involves dispersing the appropriate amount of graphene powder in dimethyl formamide solution to obtain graphene oxide dispersion having a concentration of 0.7-1.67 mg/ml, adding cobalt salt and polyvinylpyrrolidone to dispersion to obtain mixed solution, adding mixed solution into hydrothermal reactor, maintaining the filling degree of reactor at 75-80%, closing reactor in explosion-proof oven, raising temperature from room temperature to 195-220 degrees C at rate of 3-5 degrees C/minute for 20-40 hours, natural cooling to collect the precipitate in the reactor, washing, and drying. The concentration of cobalt salt in mixed solution is 0.05-0.15 M. The addition amount of polyvinylpyrrolidone is 20-30 mg per ml of dimethyl formamide solution. An INDEPENDENT CLAIM is included for lithium ion battery cathode material.