• 专利标题:   Preparing conductive graphene film comprises e.g. adding graphene oxide to deionized water to form a mixed solution, stirring and ultrasonically dispersing the mixture, and removing the bubbles in the mixed solution by vacuuming.
  • 专利号:   CN110255535-A
  • 发明人:   YANG C, REN Z, CHEN Y, HAO S, XING Y
  • 专利权人:   AECC BEIJING AERONAUTICAL MATERIALS INS
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN110255535-A 20 Sep 2019 C01B-032/184 201981 Pages: 6 Chinese
  • 申请详细信息:   CN110255535-A CN10513167 14 Jun 2019
  • 优先权号:   CN10513167

▎ 摘  要

NOVELTY - Preparing conductive graphene film comprises (i) adding graphene oxide to deionized water to form a mixed solution, stirring and ultrasonically dispersing the mixture, and removing the bubbles in the mixed solution by vacuuming to obtain a graphene oxide suspension, (ii) placing the graphene oxide suspension in a mold and performing freeze-drying treatment to obtain a graphene oxide macroscopic body having honeycomb structure, and the macroscopic bulk density is 0.0001-0.0500 g/cm3, (iii) cold pressing the graphene oxide macroscopic body, pressing the graphene oxide macroscopic body into a graphene oxide film with a film thickness of 10-100 mu m, and (iv) performing chemical reduction and thermal reduction of the graphene oxide film resulting in a graphene film having film thickness of 10-100 mu m and film density of 0.5-2500 g/m2. USE - The method is useful for preparing conductive graphene film. ADVANTAGE - The method: is simple; and produces high efficiency and large size graphene film products.