• 专利标题:   Preparing graphene oxide grafted basalt fiber multi-scale reinforcements using dopamine as endo comprises e.g. oxidized graphene ammoniating: adding the graphene oxide into deionized water, and ultrasonically dispersing.
  • 专利号:   CN107254066-A
  • 发明人:   LIU Y, ZHOU S, WANG J, WANG S, ZHAO G
  • 专利权人:   UNIV NORTH CHINA
  • 国际专利分类:   C08J005/06, C08K007/10, C08K009/02, C08K009/10, C08L077/02
  • 专利详细信息:   CN107254066-A 17 Oct 2017 C08K-009/10 201782 Pages: 10 Chinese
  • 申请详细信息:   CN107254066-A CN10450363 15 Jun 2017
  • 优先权号:   CN10450363

▎ 摘  要

NOVELTY - Preparing graphene oxide grafted basalt fiber multi-scale reinforcements using dopamine as endo comprises e.g. oxidized graphene ammoniating: adding the graphene oxide into deionized water, ultrasonically dispersing, preparing graphene oxide solution, adding quadrol, 60-120 degrees C water bath stirring for 8-24 hours, centrifuging the precipitate, washing, drying to obtain aminated graphene, dopamine-modified basalt fiber: configuring pH 7.5-10 tris hydrochloride buffer solution, adding dopamine modified basalt fiber basalt fiber, ultrasonic dispersion, adding dopamine hydrochloride. USE - The method is useful for preparing graphene oxide grafted basalt fiber multi-scale reinforcements using dopamine as endo. The graphene oxide grafted basalt fiber multi-scale reinforcement is used as reinforcements in composite materials (all claimed). ADVANTAGE - The method: improve the interfacial compatibility with the matrix in the composite material; can effectively alleviate stress concentration; inhibit composite interface damage; and improves the composite properties. DETAILED DESCRIPTION - Preparing graphene oxide grafted basalt fiber multi-scale reinforcements using dopamine as endo comprises (1) oxidized graphene ammoniating: adding the graphene oxide into deionized water, ultrasonically dispersing, preparing graphene oxide solution, adding quadrol, 60-120 degrees C water bath stirring for 8-24 hours, centrifuging the precipitate, washing, drying to obtain aminated graphene, (2) dopamine-modified basalt fiber: configuring pH 7.5-10 tris hydrochloride buffer solution, adding dopamine modified basalt fiber basalt fiber, ultrasonic dispersion, adding dopamine hydrochloride, stirring for 8-48 hours under the room temperature, washing, drying, (3) aminated graphene grafted fiber: configuring pH 7.5-10 tris hydrochloride buffer solution, step 1) adding amino-graphite alkene ultrasonic dispersion, adding obtained in the step 2), stirring for 8-48 hours under room temperature to obtain the oxide graphene graft basalt fiber multi-scale reinforcement.