• 专利标题:   Extraction of odorless white silkworm pupa oil involves crushing silkworm pupa waste, subjecting to ultrasonic-assisted organic solvent extraction, adding modified graphene oxide to crude silkworm pupa oil, and adsorbing.
  • 专利号:   CN104250582-A, CN104250582-B
  • 发明人:   CAO Y, HU Y, LI Y, PENG H
  • 专利权人:   HUNAN TRADITIONAL CHINESE MEDICINE INST
  • 国际专利分类:   C11B001/10, C11B003/00, C11B003/10
  • 专利详细信息:   CN104250582-A 31 Dec 2014 C11B-001/10 201518 Pages: 6 Chinese
  • 申请详细信息:   CN104250582-A CN10447485 04 Sep 2014
  • 优先权号:   CN10447485

▎ 摘  要

NOVELTY - Silkworm pupa waste is dried, crushed, and obtained powder is subjected to ultrasonic-assisted organic solvent extraction to obtain crude silkworm pupa oil. Modified graphene oxide is added, adsorption treatment is carried out at 10-60 degrees C for 0.25-5 hours, and filtered to obtain odorless white purified pupa oil. Modified graphene oxide is prepared by heat-treating graphite at 880-920 degrees C by Hummers method. The crude silkworm pupa oil has solid-liquid ratio of 0.1-0.6 g:10 ml. USE - Extraction of odorless white silkworm pupa oil from silkworm pupa waste (claimed). ADVANTAGE - The method enables rapid extraction of odorless white silkworm pupa oil having excellent decolorizing effect, with high purity without damaging active ingredients, by a simple process.