• 专利标题:   Method for preparing functionalized graphene loaded palladium nano-particle composite material for detecting electrode modified nitroaromatic compounds, involves graphite in water, adding pyrenetetrasulfonic acid followed by stirring.
  • 专利号:   CN103344686-A, CN103344686-B
  • 发明人:   DU J, LU X, WANG Y, YUAN C, ZHOU X
  • 专利权人:   UNIV NORTHWEST NORMAL
  • 国际专利分类:   G01N027/30
  • 专利详细信息:   CN103344686-A 09 Oct 2013 G01N-027/30 201404 Pages: 9 Chinese
  • 申请详细信息:   CN103344686-A CN10240959 18 Jun 2013
  • 优先权号:   CN10240959

▎ 摘  要

NOVELTY - A functionalized graphene loaded palladium nano-particle composite material preparing method involves dispersing graphite in water to obtain graphene suspension, adding pyrenetetrasulfonic acid with sodium hydroxide solution to the mixture, heating and stirring for 8-15 hours, filtering to obtain functional graphene. The functional graphene is dispersed in water to obtain the functional graphene suspension, followed by adding palladium chloride solution and sodium borohydride solution, heating and stirring for 8-15 hours, centrifugally filtering to obtain finished product. USE - Method for preparing functionalized graphene loaded palladium nano-particle composite material that is utilized for detecting electrode modified nitroaromatic compounds (claimed). ADVANTAGE - The method enables detecting nitro aromatic compounds with good catalytic performance, low detection lines, and high sensitivity detection of nitrobenzene.