• 专利标题:   Preparing graphene-based composite gas gel, comprises e.g. electrospinning nano-oxide precursor spinning solution, calcining, homogeneously crushing, ultrasonicating, and mixing with graphene oxide, and then ultrasonic treating, and bidirectional freezing drying.
  • 专利号:   CN115724646-A
  • 发明人:   XIE Y, WU C, WANG J, FANG Q, ZHENG K, XIA B
  • 专利权人:   UNIV SCI TECHNOLOGY CHINA ADVANCED TEC
  • 国际专利分类:   B01J020/02, B01J020/20, B01J020/28, C04B030/02
  • 专利详细信息:   CN115724646-A 03 Mar 2023 C04B-030/02 202326 Chinese
  • 申请详细信息:   CN115724646-A CN11527353 30 Nov 2022
  • 优先权号:   CN11527353

▎ 摘  要

NOVELTY - Preparing graphene-based composite gas gel, comprises (i) preparing nano-oxide precursor spinning solution, and electrospinning the nano-oxide precursor spinning solution to obtain nano-oxide fiber film, (ii) calcining the nano-oxide fiber film prepared in step (i), homogeneously crushing, and then ultrasonicating to obtain short ceramic fibers, and (iii) mixing the short ceramic fibers with graphene oxide to form solution, and then ultrasonic treating, and bidirectional freezing and drying to obtain final product. USE - The graphene-based composite airgel is useful in adsorption of oil slicks on water, sewage treatment, dye adsorption and heavy metal adsorption (claimed). ADVANTAGE - The method: utilizes nano-oxide fibers, which can enhance the mechanical strength of the aerogel; is easy to operate, low cost and simple preparation process and is suitable for large-scale preparation. The graphene oxide composite airgel has high compressibility and scalability at the same time.