• 专利标题:   High temperature-resistant nylon composite material comprises e.g. nylon salt, graphene oxide, organic nano-montmorillonite, expanded graphite, silane coupling agent KH560, nano titanium dioxide, talc and zirconium silicate.
  • 专利号:   CN107868450-A
  • 发明人:   ZHENG J, ZHANG Q, LI W
  • 专利权人:   HENAN ZHILIAN HUANYU INTELLECTUAL PROPER
  • 国际专利分类:   C08K013/06, C08K003/04, C08K003/22, C08K003/34, C08K007/24, C08L077/06
  • 专利详细信息:   CN107868450-A 03 Apr 2018 C08L-077/06 201828 Pages: 7 Chinese
  • 申请详细信息:   CN107868450-A CN10858304 28 Sep 2016
  • 优先权号:   CN10858304

▎ 摘  要

NOVELTY - High temperature-resistant nylon composite material comprises 95-105 pts. wt. nylon salt, 2-10 pts. wt. graphene oxide, 4-8 pts. wt. brucite fiber, 3-8 pts. wt. expanded graphite, 2-6 pts. wt. silane coupling agent KH560, 1-4 pts. wt. 20-25% solid containing carbon dioxide sols, 1-4 pts. wt. nano titanium dioxide, 1-3 pts. wt. talc, 1-3 pts. wt. organic nano-montmorillonite, 0.5-1 pts. wt. zirconium silicate, 0.2-1 pts. wt. blocking agent, 0.1-0.6 pts. wt. 6-aminocaproic acid and 40-70 pts. wt. deionized water. USE - Used as high temperature-resistant nylon-graphene composite material. ADVANTAGE - The composite material: has excellent flame retardancy, high temperature resistance, wear resistance and mechanical property. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for preparing high temperature-resistant nylon composite material comprising (i) mixing nylon salt, graphene oxide, blocking agents and 6-aminocaproic acid, ultrasonically dispersing at 50-85 degrees C for 1-3 hours to obtain premix and adding premix into autoclave, (ii) adding nano carbon sol with a solid content of 20-25%, brucite fiber, expanded graphite, silane coupling agent KH560, nano titanium dioxide, talc, zirconium silicate and organic nanometer montmorillonite into deionized water, mixing ultrasonically, adding into the high pressure reactor, and (iii) replacing air in the autoclave by nitrogen for three times, where nitrogen gas is used as a reaction protective gas, heating at 160-260 degrees C, pressure of 2-3.5 MPa, maintaining pressure at 2-3.5 MPa by releasing water vapor in the reactor for 1-3 hours, releasing pressure in the reactor to atmospheric pressure, discharging and temperature in the kettle does not exceed 280 degrees C.