• 专利标题:   Preparation of graphene-based carboxymethyl cellulose nanocrystalline composite material, by mixing graphene oxide dispersion, aqueous solution of sodium carboxymethyl cellulose and ethylenediamine, filtering and drying filtrate.
  • 专利号:   CN108152353-A
  • 发明人:   MO Z, WANG R, ZHANG H, YAN M, FENG H, LI Z, NIU X, GUO R
  • 专利权人:   UNIV NORTHWEST NORMAL
  • 国际专利分类:   G01N027/30, G01N027/48
  • 专利详细信息:   CN108152353-A 12 Jun 2018 G01N-027/48 201858 Pages: 8 Chinese
  • 申请详细信息:   CN108152353-A CN11494563 31 Dec 2017
  • 优先权号:   CN11494563

▎ 摘  要

NOVELTY - Preparation of graphene-based Carboxymethyl cellulose nanocrystalline composite material involves ultrasonically dispersing graphene oxide in ultrapure water, adding 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride as carbonyl activator, ultrasonically processing for 20-25 minutes to form graphene oxide dispersion, dispersing sodium carboxymethyl cellulose in ultrapure water, adding 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride as carbonyl activator, stirring uniformly to form aqueous solution of sodium carboxymethyl cellulose, mixing carboxymethyl cellulose sodium aqueous solution with graphene oxide dispersion, adding ethylenediamine and crosslinker including N-hydroxysuccinimide, reacting at 48-55 degrees C for 50-53 hours, adding hydrazine hydrate to reduce excess oxygen-containing functional groups and carbon-oxygen double bonds on the graphene oxide, suction-filtering, washing filtrate and drying. USE - Preparation of graphene-based carboxymethyl cellulose nanocrystalline composite material. ADVANTAGE - The method enables simple and rapid preparation of graphene-based carboxymethyl cellulose nanocrystalline composite material.