• 专利标题:   Manufacture of tough graphene-cellulose composite thermal conductive film for functional composite material, involves adding cellulose aqueous solution to graphene solution, ultrasonically treating and performing self-assembly remodeling.
  • 专利号:   CN107293377-A
  • 发明人:   WANG F
  • 专利权人:   UNIV QILU TECHNOLOGY
  • 国际专利分类:   H01B001/24, H01B013/00
  • 专利详细信息:   CN107293377-A 24 Oct 2017 H01B-013/00 201781 Pages: 8 Chinese
  • 申请详细信息:   CN107293377-A CN10548856 07 Jul 2017
  • 优先权号:   CN10548856

▎ 摘  要

NOVELTY - Manufacture of tough graphene-cellulose composite thermal conductive film involves adding nano-cellulose aqueous solution to a graphene aqueous solution, ultrasonically treating to obtain uniformly dispersed graphene/cellulose mixture, performing vacuum filtration using a microporous membrane, performing self-assembly remodeling to form a graphene and cellulose membrane, washing, drying at room temperature for 24 hours, processing in vacuum oven for 12-24 hours at 50-100 degrees C, and hot pressing. USE - Manufacture of tough graphene-cellulose composite thermal conductive film for functional composite material. ADVANTAGE - The graphene-cellulose composite film having excellent thermal conductivity, electroconductivity, mechanical properties and electrical properties is produced economically by simple method. DETAILED DESCRIPTION - Manufacture of tough graphene-cellulose composite thermal conductive film involves adding graphene and a dispersant to a solvent, producing a graphene solution having concentration of 0.2-5 mg/ml, ultrasonically treating to obtain uniformly dispersed graphene suspension, dispersing wood pulp in an aqueous solution, shearing in liquid phase in a homogenizer, dispersing cellulose into individual fiber bundles, mixing deionized water, dispersing using a high-speed shearing machine to obtain a nano-cellulose aqueous solution, adding resulting solution to the graphene aqueous solution, ultrasonically treating to obtain uniformly dispersed graphene/cellulose mixture, performing vacuum filtration using a microporous membrane, performing self-assembly remodeling to form a graphene and cellulose membrane, washing, drying at room temperature for 24 hours, processing in vacuum oven for 12-24 hours at 50-100 degrees C, and hot pressing.