• 专利标题:   Graphene or hydroxyapatite composite material preparation involves uniformly mixing graphene oxide solution or suspension and calcium ion to obtain mixed solution A, is simple and ecofriendly.
  • 专利号:   CN103420364-A, CN103420364-B
  • 发明人:   ZHANG M, LU X, PENG Z, WANG X, WENG J
  • 专利权人:   UNIV SOUTHWEST JIAOTONG
  • 国际专利分类:   C01B025/32, C01B031/04
  • 专利详细信息:   CN103420364-A 04 Dec 2013 C01B-031/04 201414 Pages: 8 Chinese
  • 申请详细信息:   CN103420364-A CN10296678 13 Jul 2013
  • 优先权号:   CN10296678

▎ 摘  要

NOVELTY - Graphene-hydroxyapatite composite material preparation involves uniformly mixing 0.0l-3.0 mol/l graphene oxide solution or suspension and 0.5-5 mg/ml calcium ion to obtain a mixed solution A. Calcium and phosphorus are mixed in combined solution in molar ratio of 1.5-2.0:1, then 0.01-2.0mol/l phosphate are mixed and stirred by a magnetic stirrer to obtain a product. Mixed solution A is added into obtained product, and then uniformly mixed to obtain a solution. pH of obtained solution is adjusted by using pH adjusting agent to 8-14. USE - Method for preparing graphene-hydroxyapatite composite material (claimed). ADVANTAGE - The method enables preparing graphene-hydroxyapatite composite material with high mechanical strength and retaining bone activity at industrial level in a simple and eco-friendly manner. DETAILED DESCRIPTION - Graphene-hydroxyapatite composite material preparation involves uniformly mixing 0.0l-3.0 mol/l graphene oxide solution or suspension and 0.5-5 mg/ml calcium ion to obtain a mixed solution A. Calcium and phosphorus are mixed in combined solution in molar ratio of 1.5-2.0:1, then 0.01-2.0mol/l phosphate are mixed and stirred by a magnetic stirrer to obtain a product. Mixed solution A is added into obtained product, and then uniformly mixed to obtain a solution. pH of obtained solution is adjusted by using pH adjusting agent to 8-14. The mixed liquid is transferred into autoclave at 160-240 degrees C for 12 hours under hydrothermal treatment.