• 专利标题:   Preparation of low-cost large area graphene transparent conductive film for electronic material, by dispersing graphene oxide or graphite chip in solvent, coating solution on substrate, recrystallizing at high temperature, and cooling.
  • 专利号:   CN102815695-A
  • 发明人:   XU Z
  • 专利权人:   XU Z
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102815695-A 12 Dec 2012 C01B-031/04 201345 Pages: 5 Chinese
  • 申请详细信息:   CN102815695-A CN10273075 02 Aug 2012
  • 优先权号:   CN10273075

▎ 摘  要

NOVELTY - Preparation of a low-cost large area graphene transparent conductive film comprises dispersing a graphene oxide or graphite chip in a solvent to obtain 0.01-10 mass% solution; coating the solution on a substrate, volatilizing the solvent, and uniformly adhering the graphene oxide or graphite chip on the substrate; placing the film in an oxygen molecule and in a cavity under the protection of an inert gas, heating to 500-1500 degrees C, and recrystallizing at high temperature; cooling to room temperature; and transferring the graphene film to the transparent substrate. USE - Method for the preparation of a low-cost large area graphene transparent conductive film used for an electronic material. ADVANTAGE - The method uses high temperature recrystallization method to replace the traditional chemical vapor deposition method, thus avoiding the use of expensive high purity gas source. DETAILED DESCRIPTION - Preparation of a low-cost large area graphene transparent conductive film comprises: (A) dispersing a graphene oxide or graphite chip in a solvent to obtain 0.01-10 mass% solution; (B) coating the solution on a substrate, volatilizing the solvent, and uniformly adhering the graphene oxide or graphite chip on the substrate; (C) placing the film in an oxygen molecule and in a cavity under the protection of an inert gas, heating to 500-1500 degrees C, keeping high temperature for more than 10 minutes, and recrystallizing at high temperature; (D) quickly cooling to room temperature at 200 degrees C/minute; and (E) transferring the graphene film to the transparent substrate.