• 专利标题:   Preparation of low temperature-resistant composite material by reacting dipropylene glycol diacrylate, succinic anhydride and m-phenylene diisocyanate, and mixing with lignin, propylene glycol methyl ether acetate and graphene oxide.
  • 专利号:   CN105001826-A
  • 发明人:   DANG B
  • 专利权人:   SUZHOU KEMIAO NEW MATERIALS CO LTD
  • 国际专利分类:   C08G018/76, C09J011/04, C09J011/06, C09J011/08, C09J169/00, C09J175/04
  • 专利详细信息:   CN105001826-A 28 Oct 2015 C09J-175/04 201637 Pages: 6 Chinese
  • 申请详细信息:   CN105001826-A CN10409784 14 Jul 2015
  • 优先权号:   CN10409784

▎ 摘  要

NOVELTY - Preparation of low temperature-resistant composite material comprises reacting dipropylene glycol diacrylate, succinic anhydride and m-phenylene diisocyanate to obtain resin prepolymer, mixing lignin, polyoxyethylene sorbitan monooleate and propylene glycol methyl ether acetate to obtain mixture, taking graphene oxide and hydrazine hydrate, adding mixture, stirring, adding silver ammonia solution, pyridine-nitrobenzoic acid salt, stirring, adding trimethylene carbonate and polyethylene glycol monomer, stirring, adding resin prepolymer, stirring, entering to mold and mold-pressing. USE - Method for preparing low temperature-resistant composite material (claimed). ADVANTAGE - The composite material has excellent mechanical property, good curing effect, stable structure and increased anti-brittleness property. DETAILED DESCRIPTION - Preparation of low temperature-resistant composite material comprises reacting dipropylene glycol diacrylate, succinic anhydride and m-phenylene diisocyanate at 150 degrees C for 70 minutes to obtain resin prepolymer, mixing lignin, polyoxyethylene sorbitan monooleate and propylene glycol methyl ether acetate for 2 hours to obtain mixture, taking graphene oxide and hydrazine hydrate, adding mixture, stirring for 4 hours, adding silver ammonia solution, pyridine-nitrobenzoic acid salt, stirring at 60 degrees C for 8 hours, adding trimethylene carbonate and polyethylene glycol monomer, stirring at 105 degrees C for 3 hours, adding resin prepolymer, stirring at 80 degrees C for 4 hours, entering to mold and mold-pressing.