• 专利标题:   Preparation of monolayer graphene oxide involves mixing graphite and acid, stirring, reacting, adding ferrate oxidizing agent and stabilizer, stripping, centrifuging, adding to deionized water, precipitating, washing and centrifuging.
  • 专利号:   CN104310385-A, WO2016054877-A1
  • 发明人:   GAO C, SUN H, XU Z, ZHENG Y, PENG L, WEI Y
  • 专利权人:   ZHEJIANG TANGU SHANGXI MATERIAL TECHNOLO, ZHEJIANG TANGU SHANGXI MATERIAL SCI TEC
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104310385-A 28 Jan 2015 C01B-031/04 201527 Pages: 7 Chinese
  • 申请详细信息:   CN104310385-A CN10526910 09 Oct 2014
  • 优先权号:   CN10526910

▎ 摘  要

NOVELTY - Preparation of monolayer graphene oxide involves mixing graphite and acid, stirring, reacting at -10 to 20 degrees C for 5 minutes to 1 hour, adding ferrate oxidizing agent and stabilizer, reacting at -10 to 80 degrees C for 0.5-24 hours, stripping, centrifuging, discharging acid, adding remainder product to deionized water, precipitating, washing precipitate using dilute hydrochloric acid and deionized water and centrifuging. USE - Preparation of monolayer graphene oxide (claimed). ADVANTAGE - The method enables simple and environmentally-friendly preparation of monolayer graphene oxide with reduced energy consumption, without using heavy metal.