• 专利标题:   Manufacture of carbon nanowall for graphene nanobelt, involves etching metal substrate using acid solution, heating etched metal substrate, irradiating ultraviolet ray, reacting, and supplying carbon-containing gas and protective gas.
  • 专利号:   CN103935975-A, CN103935975-B
  • 发明人:   WANG Y, WU F, YUAN X, ZHOU M
  • 专利权人:   OCEANS KING LIGHTING SCI TECHNOLOGY CO, SHENZHEN OCEANS KING LIGHTING ENG CO LTD, SHENZHEN OCEANS KING LIGHTING SCI TECH
  • 国际专利分类:   B82Y030/00, C01B031/02, C01B031/04
  • 专利详细信息:   CN103935975-A 23 Jul 2014 C01B-031/02 201468 Pages: 15 Chinese
  • 申请详细信息:   CN103935975-A CN10019410 18 Jan 2013
  • 优先权号:   CN10019410

▎ 摘  要

NOVELTY - Manufacture of carbon nanowall involves etching metal substrate using acid solution having concentration of 0.01-1 mol/L for 0.5-10 minutes, heating etched metal substrate at 600-900 degrees C under anaerobic condition, irradiating ultraviolet ray to metal substrate surface, reacting, and supplying carbon-containing gas and protective gas for 30-300 minutes. The flow rate of carbon-containing gas is 10-1000 sccm. The ratio of flow rate of carbon-containing gas and protective gas is 2-10:1. USE - Manufacture of carbon nanowall used for manufacturing graphene nanobelt (claimed). ADVANTAGE - The method enables manufacture of carbon nanowall having uniform wall thickness and complete structure. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for manufacture of graphene nanobelt, which involves mixing carbon nanowall and chloride intercalating agent, heating at 460-550 degrees C for 2-6 hours, ultrasonically-treating for 3-24 hours and filtering.