• 专利标题:   Preparation of airgel graphene by heating oxidized graphene, adding aqueous solution of sodium ion and bicarbonate ion, heating, soaking in deionized water, heating, leaching or dialyzing, and freeze-drying or supercritical drying.
  • 专利号:   CN103991864-A, CN103991864-B
  • 发明人:   WANG G, YANG S, ZHU W
  • 专利权人:   UNIV CHINA SCI TECHNOLOGY
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103991864-A 20 Aug 2014 C01B-031/04 201475 Pages: 9 Chinese
  • 申请详细信息:   CN103991864-A CN10210432 16 May 2014
  • 优先权号:   CN10210432

▎ 摘  要

NOVELTY - Preparation of airgel graphene comprises heating oxidized graphene; adding aqueous solution of sodium ion (Na+) and bicarbonate ion (HCO3-) to obtain hydrogel; heating hydrogel at 100-150 degrees C to obtain graphene hydrogel; soaking graphene hydrogel in deionized water; heating at stable temperature of 50-99 degrees C for 0.5-3 hours; conducting leaching or dialysis process to graphene hydrogel; freeze-drying or supercritical drying; and removing water in graphene hydrogel. USE - Method for preparing airgel graphene (claimed). ADVANTAGE - The method is simple; has mild reaction condition; uses non-toxic, pollution-free and easy to obtain raw material; and has low cost.