• 专利标题:   Preparing electrochromatic material involves dispersing carboxyl group graphene in dimethyl formamide in water bath under ultrasonic dispersion in protection of inert gas.
  • 专利号:   CN104630817-A, CN104630817-B
  • 发明人:   XU K, WU X, ZHANG W
  • 专利权人:   UNIV XIAN TECHNOLOGICAL
  • 国际专利分类:   C01B031/04, C25B003/00, C01B032/184
  • 专利详细信息:   CN104630817-A 20 May 2015 C25B-003/00 201558 Pages: 7 Chinese
  • 申请详细信息:   CN104630817-A CN10796369 18 Dec 2014
  • 优先权号:   CN10796369

▎ 摘  要

NOVELTY - Electrochromatic material preparation involves dispersing carboxyl group graphene in dimethyl formamide in water bath under ultrasonic dispersion in protection of an inert gas for 1 hour at 50 degrees C. The resultin mixture is heated with toluene diisocyanate for 24 hours to remove isocyanate groups. The removed isocyanate groups are modified with graphene, 4-amino-6-hydroxy-2-methylpyrimidine and triethyl acetate in dimethylformamide to give 2-ureido-4(1H)-pyrimidinone. USE - Method for preparing electrochromatic material (claimed). ADVANTAGE - The method prepares electrochromatic material in a simple manner with increased dispersing and electrochromic properties, and large surface area. DETAILED DESCRIPTION - Electrochromatic material preparation involves dispersing carboxyl group graphene in dimethyl formamide in water bath under ultrasonic dispersion in protection of an inert gas for 1 hour at 50 degrees C. The resulting mixture is heated with toluene diisocyanate for 24 hours to remove isocyanate groups. The removed isocyanate groups are modified with graphene, 4-amino-6-hydroxy-2-methylpyrimidine and triethyl acetate in dimethylformamide to give 2-ureido-4(1H)-pyrimidinone. The formed mixture is heated at 100 degrees C under ultrasonic agitation for 20 hours, and then dried to obtain hydrogen bonded graphene dispersion solution.