• 专利标题:   Preparing graphene/polymer hybrid material comprises adding graphene oxide to flask and then dispersing in solvent A, and adding dispersed graphene oxide and triethylamine and then reacting and drying.
  • 专利号:   CN103204978-A, CN103204978-B
  • 发明人:   SHEN T, WANG J, YUAN W
  • 专利权人:   UNIV TONGJI
  • 国际专利分类:   C08F220/34, C08F292/00, C08F008/44
  • 专利详细信息:   CN103204978-A 17 Jul 2013 C08F-292/00 201424 Pages: 9 Chinese
  • 申请详细信息:   CN103204978-A CN10113730 03 Apr 2013
  • 优先权号:   CN10113730

▎ 摘  要

NOVELTY - Preparing graphene/polymer hybrid material comprises adding graphene oxide to a flask and then dispersing in a solvent A, adding the dispersed graphene oxide and triethylamine and then reacting and drying in a vacuum, adding the obtained halogenated graphene oxide with methacrylic acid and N,N-dimethylaminoethyl methacrylate into a solvent B and then reacting, drying the mixture to dilute, centrifuging the mixture, adding the obtained product with tetrahydrofuran and 1,3-propanesultone in the hybrid material and then reacting and washing, and drying the mixture. USE - The method is useful for preparing graphene/polymer hybrid material (claimed). ADVANTAGE - The method simply provides the graphene/polymer hybrid material with good temperature sensitivity in a simple manner. DETAILED DESCRIPTION - Preparing graphene/polymer hybrid material comprises (a) adding graphene oxide to a flask and then dispersing in a solvent A, adding halogenated compound of graphene oxide and triethylamine and then reacting at 10 degrees C for 24-48 hours and drying in a vacuum to obtain halogenated graphene oxide, (b) adding the obtained halogenated graphene oxide with methacrylic acid and N,N-dimethylaminoethyl methacrylate into a solvent B and then reacting at a temperature of 40-80 degrees C for 12-48 hours, and drying the mixture to dilute, centrifuging the mixture to obtain a product, and (c) adding the obtained product with tetrahydrofuran and 1,3-propanesultone in the catalyst C and then reacting at room temperature for 20-48 hours and washing, and drying the mixture.