• 专利标题:   Preparation of doped tin oxide composite conductive film involves spraying graphene-containing mixture onto surface of substrate, spraying mixed solution containing tin tetrachloride, dopant and organic solvent, and annealing.
  • 专利号:   CN108615585-A
  • 发明人:   ZHU K, HE S, HOU H, DAI H, WU Q
  • 专利权人:   YANCHENG INST TECHNOLOGY
  • 国际专利分类:   H01B013/00
  • 专利详细信息:   CN108615585-A 02 Oct 2018 H01B-013/00 201875 Pages: 6 Chinese
  • 申请详细信息:   CN108615585-A CN10468090 15 May 2018
  • 优先权号:   CN10468090

▎ 摘  要

NOVELTY - Preparation of doped tin oxide composite conductive film involves dissolving 0.5-0.9 mol/L tin tetrachloride and dopant in an organic solvent containing ethanol and/or dimethylformamide to obtain a mixed solution, leaving still for 10-20 hours, adding graphene, ultrasonically dispersing to obtain mixed solution containing graphene, spraying graphene-containing mixture onto the surface of the substrate through an ultrasonic spray pyrolysis coating machine, spraying a mixed solution, and annealing under argon atmosphere. The dopant comprises lanthanum nitrate-antimony trichloride, yttrium nitrate-antimony trichloride or cerium nitrate-antimony trichloride. The molar ratio of lanthanum nitrate, yttrium nitrate and cerium nitrate to antimony trichloride is 0.1-1:1. USE - Preparation of doped tin oxide composite conductive film. ADVANTAGE - The method is simple and easy to control, and provides conductive film having excellent conductive effect, uniform surface and compact structure.