• 专利标题:   Method for preparing graphene hydrogen storage electrode, involves utilizing hydrogen direct current electric arc plasma apparatus and preparing graphene material by utilizing graphite block as anode and carbon rod as cathode.
  • 专利号:   CN102623668-A
  • 发明人:   DONG X, GUO G, HUANG H, QUAN X, XUE F
  • 专利权人:   UNIV DALIAN TECHNOLOGY
  • 国际专利分类:   H01M004/04
  • 专利详细信息:   CN102623668-A 01 Aug 2012 H01M-004/04 201322 Pages: 8 Chinese
  • 申请详细信息:   CN102623668-A CN10093707 31 Mar 2012
  • 优先权号:   CN10093707

▎ 摘  要

NOVELTY - A graphene hydrogen storage electrode preparation method involves utilizing automatic control hydrogen direct current electric arc plasma apparatus, preparing graphene material by utilizing a graphite block as anode, carbon rod as cathode, metering 10-30 mm as two inter-electrode distance, maintaining vacuum pressure, mixing graphene and polyvinylidene difluoride binder, coating and pressing to obtain electrode plate, utilizing electrochemical hydrogen storage test of a three-electrode system as auxiliary electrode, nickel compound electrode and calomel electrode as a reference electrode. USE - Method for preparing a graphene hydrogen storage electrode. ADVANTAGE - The method enables preparing a graphene hydrogen storage electrode in an inexpensive manner. DETAILED DESCRIPTION - A graphene hydrogen storage electrode preparation method involves utilizing automatic control hydrogen direct current electric arc plasma apparatus, preparing graphene material by utilizing graphite block as anode, carbon rod as cathode, metering 10-30 mm as two inter-electrode distance, maintaining 0.01-0.07 MPa of vacuum pressure, mixing graphene and polyvinylidene difluoride binder in a mass ratio of 1:1-7:1, coating and pressing to obtain electrode plate, utilizing electrochemical hydrogen storage test of three-electrode system as auxiliary electrode, nickel compound (Ni(OH)2/NiOOH) electrode and calomel electrode as reference electrode.