• 专利标题:   Rapid thermal processing method for preparing graphene powder in air atmosphere comprises putting precursor of graphene in non-sealing cover crucible, then carrying out heat treatment to obtain graphene powder.
  • 专利号:   CN103072977-A, WO2014117434-A1
  • 发明人:   DING G, JIANG M, LI X, SUN J, XIE X
  • 专利权人:   CHINESE ACAD SCI SHANGHAI MICROSYSTEM, SHANGHAI INST MICROSYSTEM INFORMATION
  • 国际专利分类:   C01B031/04, C01B031/02
  • 专利详细信息:   CN103072977-A 01 May 2013 C01B-031/04 201379 Pages: 14 Chinese
  • 申请详细信息:   CN103072977-A CN10036671 30 Jan 2013
  • 优先权号:   CN10036671

▎ 摘  要

NOVELTY - A rapid thermal processing method for preparing graphene powder in air atmosphere comprises putting precursor of graphene in non-sealing cover crucible, then carrying out heat treatment in the air atmosphere to obtain the graphene powder. USE - A rapid thermal processing method for preparing graphene powder in air atmosphere. ADVANTAGE - The method does not need inert gas or reducing gas. The heat treatment temperature of the graphene is reduced to 250-850 degrees C, which greatly expands the heat treatment temperature range of the graphene, and reduces the energy consumption. Nitrogen doping can be controlled (preferably at 0.62-8.96 at.%), which is good for expanding the graphene powder. The obtained graphene has 1-5 graphene layers, specific surface area of 500-918 m2/ g, and resistivity of 0.02-0.04 Omega -cm.