• 专利标题:   Graphene slurry used in preparation of conductive ink for printed circuit, is prepared by using raw materials comprising graphene which is obtained by using electrolyte containing sulfuric acid and sulfate, divalent acid ester, and ethanol.
  • 专利号:   CN110698924-A
  • 发明人:   LI J, LI W, WANG J, LIU J, LIU D, WANG X
  • 专利权人:   BEIJING GRAPHENE TECHNOLOGY RES INST CO
  • 国际专利分类:   C09D011/52
  • 专利详细信息:   CN110698924-A 17 Jan 2020 C09D-011/52 202016 Pages: 14 Chinese
  • 申请详细信息:   CN110698924-A CN10974581 14 Oct 2019
  • 优先权号:   CN10974581

▎ 摘  要

NOVELTY - Graphene slurry is prepared by using raw materials comprising 1.5 g graphene, 20-100 mL divalent acid ester, and 50-250 mL ethanol. The graphene is prepared by (1) using electrolyte containing sulfuric acid and sulfate, (2) using graphite as positive electrode placed in the electrolyte, applying a working voltage to peel the graphite, obtaining a suspension, (3) removing the liquid portion in the suspension, washing and ultrasonically processing to obtained solid portion, cooling to -100 degrees C to -60 degrees C for 2-8 hours, and treating at -56 degrees C to -44 degrees C for 35-55 hours. USE - Graphene slurry used in preparation of conductive ink (claimed) for printed circuit. ADVANTAGE - The graphene slurry provides conductive ink with high stability, printability and conductivity. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for the following: (1) preparation of graphene slurry, which involves mixing graphene, divalent acid ester and ethanol, homogenizing, and removing ethanol; (2) use of graphene slurry for preparing conductive ink; (3) conductive ink, which comprises the graphene slurry and an organic co-solvent which is added in an amount of 0.05-200 times based on the mass of the graphene slurry; and (4) preparation of conductive ink, which involves mixing raw materials.