• 专利标题:   Synthesis of boron-nitrogen co-doped graphene quantum dots includes dissolving graphene oxide and boric acid in ultrapure water, performing ultrasonic treatment, reacting, cooling, filtering, recovering reduced graphene oxide and drying.
  • 专利号:   CN110294471-A
  • 发明人:   MO Z, LIU Z, LIU N, GUO R, NIU X, YANG X, ZHAO P, OUYANG M
  • 专利权人:   UNIV NORTHWEST NORMAL
  • 国际专利分类:   C01B032/184, C09K011/63, C09K011/65
  • 专利详细信息:   CN110294471-A 01 Oct 2019 C01B-032/184 201984 Pages: 8 Chinese
  • 申请详细信息:   CN110294471-A CN10564671 27 Jun 2019
  • 优先权号:   CN10564671

▎ 摘  要

NOVELTY - Synthesis of boron-nitrogen co-doped graphene quantum dots comprises dissolving graphene oxide and boric acid in ultrapure water, adding ammonia water in ultrapure water, performing ultrasonic treatment for 10-30 minutes, transferring mixed solution in high-pressure kettle, heating for 4-20 hours at 175-180 degrees C, reacting, cooling to room temperature to obtain light yellow supernatant of boron-nitrogen co-doped graphene quantum dots and reduced graphene oxide lower sediment, filtering, recovering reduced graphene oxide, placing light yellow supernatant in dialysis bag, performing dialysis for 2-3 days, performing rotary evaporation concentration on dialysate to obtain high-concentration boron-nitrogen co-doped graphene quantum dots and drying. USE - The method is for synthesis of boron-nitrogen co-doped graphene quantum dots. ADVANTAGE - The method is environmental friendly and has simple process, mild reaction conditions and low synthesis cost.