• 专利标题:   Preparing carbon nanotube printing electrode involves adding super-dispersant direct current, water, stirring and dissolving, adding carbon nano-tube, dispersing, grinding, adding graphene nanometre sheet, and mixing.
  • 专利号:   CN114518393-A
  • 发明人:   ZHU W, ZHU A
  • 专利权人:   UNIV YANGZHOU
  • 国际专利分类:   B82Y015/00, B82Y040/00, G01N027/30, G01N027/327
  • 专利详细信息:   CN114518393-A 20 May 2022 G01N-027/30 202288 Chinese
  • 申请详细信息:   CN114518393-A CN10134187 14 Feb 2022
  • 优先权号:   CN10134187

▎ 摘  要

NOVELTY - Preparing carbon nanotube (CNT) printing electrode involves (a) adding 2-5 pts. wt. super-dispersant DC-02, 75-80 pts. wt. water, stirring and dissolving, adding 1.4-2.3 pts. wt. carbon nano-tube, dispersing for 10-15 minutes at a rotating speed of 1500 revolutions/minutes, grinding for 6-7 hours, adding 16-18 pts. wt. graphene nanosheet, continuously grinding for 10 hours after finishing, adding the graphene carbon nano-tube nanometre suspension; (b) mixing 82-85 pts. wt. graphene/carbon nanotubes nano suspension, 15-18 pt. aqueous acrylic resin, 0.1-0.3 pts. wt.leveling agent, and 0. 1-0.3 pts. wt. wetting dispersant to obtain nano coating; and (c) coating the nano coating on the working electrode of the carbon printing electrode by a dispensing machine, the thickness of the wet film is 9-13 m, drying to obtain the modified printing electrode of the graphene carbon nano-tube nano coating, namely GNP-CNT printing electrode. USE - Method for preparing carbon nanotube (CNT) printing electrode, where the GNP-CNT printing electrode is used for measuring the dopamine by the electrochemical work station (claimed). ADVANTAGE - The carbon nano technology for simply constructing the working electrode, the prepared printing electrode can quickly detect the dopamine in the blood, well overcomes the disadvantages of expensive cost, low sensitivity. The method is simple, the raw material is easy to obtain, and it has characteristics: the CNT is distributed between the GNP nano sheet in a monodisperse state, forming the three-dimensional conductive network structure shape of nano-tube bridged nano sheet, which is good for forming a high electronic transmission channel; the micro-nano surface is formed to have a large ratio surface which can effectively increase the electrode reaction rate; CNT and GNP has a large structure and the detection substance DA can form electron donor-electron acceptor interaction. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a GNP-CNT printed electrode prepared by the preparation method.