• 专利标题:   Preparing graphite oxide-loaded bismuth tungstate-based photocatalyst by dispersing sodium oleate, bismuth III nitrate pentahydrate and sodium tungstate dehydrate in ethylene glycol solution, adding graphene oxide and reacting mixture.
  • 专利号:   CN107537468-A
  • 发明人:   DAI J, DAI Q, WANG C
  • 专利权人:   ZHANGJIAGANG YANGSHE SCREEN PRINTING FAC
  • 国际专利分类:   B01J023/31, C02F001/30, C02F001/72, C02F101/30, C02F103/34
  • 专利详细信息:   CN107537468-A 05 Jan 2018 B01J-023/31 201808 Pages: 5 Chinese
  • 申请详细信息:   CN107537468-A CN10480357 27 Jun 2016
  • 优先权号:   CN10480357

▎ 摘  要

NOVELTY - Method for preparing graphite oxide-loaded bismuth tungstate-based photocatalyst involves (a) ultrasonically dispersing sodium oleate, bismuth(III) nitrate pentahydrate and sodium tungstate dehydrate in ethylene glycol solution to obtain mixed solution (A), (b) adding graphene oxide to mixed solution (A) and stirring and mixing evenly, (c) reacting mixed solution obtained in step (b) in a hydrothermal reactor and (d) ultrasonically washing the reactant obtained in step (c), drying and crushing dried mixture. USE - The method is useful for preparing graphite oxide-loaded bismuth tungstate-based photocatalyst (claimed). ADVANTAGE - The prepared graphite oxide-loaded bismuth tungstate-based photocatalyst degrades organic pollutants rate of 99% or more and exhibits rhodamine B (RhB) removal rate of 90% or more. DETAILED DESCRIPTION - Method for preparing graphite oxide-loaded bismuth tungstate-based photocatalyst involves (a) ultrasonically dispersing sodium oleate, bismuth(III) nitrate pentahydrate and sodium tungstate dehydrate in ethylene glycol solution to obtain mixed solution (A), (b) adding 3-5% graphene oxide to mixed solution (A) and stirring and mixing evenly, (c) reacting the mixed solution obtained in step (b) in a hydrothermal reactor at 200-220 degrees C for 22-24 hours and (d) ultrasonically washing the reactant obtained in step (c), drying and crushing to obtain bismuth tungstate/bismuth oxide photocatalyst supported with graphene oxide.