• 专利标题:   Preparation of graphene material by taking graphite electrode, using electrolytic solution containing N-methylpyrrolidone hydrosulfate and 1-methylimidazole hydrogen sulfate, grinding, centrifuging, and carrying out sedimentation.
  • 专利号:   CN103451670-A, CN103451670-B
  • 发明人:   LIU H, MAO M
  • 专利权人:   UNIV CENT SOUTH
  • 国际专利分类:   C25B001/00
  • 专利详细信息:   CN103451670-A 18 Dec 2013 C25B-001/00 201416 Pages: 6 Chinese
  • 申请详细信息:   CN103451670-A CN10411276 11 Sep 2013
  • 优先权号:   CN10411276

▎ 摘  要

NOVELTY - A graphene material is prepared by taking graphite electrode as negative and positive electrodes, using electrolytic solution containing 1-butyl-3-methylimidazolium dibutyl phosphate, N-methylpyrrolidone hydrosulfate, ammonium dihydrogen phosphate and 1-methylimidazole hydrogen sulfate, adding expanded graphite at ratio of 100:1-30, grinding for 3 hours, treating with mixed solution of acetone and dimethyl formamide, centrifuging at 13000 revolutions/minute, and carrying out sedimentation. USE - Method for preparing graphene material (claimed). ADVANTAGE - The method has simple and mild process conditions with high quality graphene product.