• 专利标题:   Preparing phosphorus/porous carbon/graphene composite material involves adding nano phosphorus to solvent, ultrasonically pretreating, followed by adding e.g. saccharide, ultrasonically dispersing, freeze-drying and carbonizing.
  • 专利号:   CN108767209-A
  • 发明人:   LIAN P, LIU H, MEI Y, WANG Q, CHEN J
  • 专利权人:   UNIV KUNMING SCI TECHNOLOGY
  • 国际专利分类:   H01M004/36, H01M004/38, H01M004/62, H01M010/0525, H01M010/054
  • 专利详细信息:   CN108767209-A 06 Nov 2018 H01M-004/36 201902 Pages: 14 Chinese
  • 申请详细信息:   CN108767209-A CN10384321 26 Apr 2018
  • 优先权号:   CN10384321

▎ 摘  要

NOVELTY - Preparing phosphorus/porous carbon/graphene composite material involves: (1) adding nano phosphorus to a solvent at 5-30 degrees C and then carrying out ultrasonic pretreatment or shear pretreatment to obtain nano phosphorus dispersion, where the solvent is water, an ionic liquid or an organic solvent; (2) adding a saccharide or graphene oxide to the nano phosphorus dispersion obtained in step (1) and performing ultrasonic dispersion treatment for 0.5-3 hours to obtain a mixed dispersion; (3) subjecting the mixed dispersion obtained in step (2) to low-temperature freeze-drying to obtain a phosphorus/sugar/graphene oxide solid foam; and (4) subjecting the phosphorus/sugar/graphene oxide solid foam obtained in step (3) to a high-temperature carbonization treatment at 600-1000 degrees C for 1-8 hours under an inert gas atmosphere. USE - The method is useful for preparing phosphorus/porous carbon/graphene composite material. ADVANTAGE - The method prepares phosphorus/porous carbon/graphene composite material with high conductivity, excellent distribution uniformity of phosphorus and carbon and sandwich porous structure. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for the phosphorus/porous carbon/graphene composite material prepared by the above method.