• 专利标题:   Preparing selective oxidation catalyst, involves using water solution containing nitrogen element to dip carbon-containing material, mixing nitrogen-doped carbon carrier with active metal component compound solution, performing first drying and first reduction to first mixture.
  • 专利号:   CN115722241-A
  • 发明人:   ZONG B, RONG J, DU Z, CHEN G, SUN Q, ZHAO H, ZHENG L
  • 专利权人:   RES INST PETROLEUM PROCESSING SINOPEC, CHINA PETROLEUM CHEM CORP
  • 国际专利分类:   B01J027/24, B01J035/10, C07D307/46
  • 专利详细信息:   CN115722241-A 03 Mar 2023 B01J-027/24 202323 Chinese
  • 申请详细信息:   CN115722241-A CN10991167 26 Aug 2021
  • 优先权号:   CN10991167

▎ 摘  要

NOVELTY - Preparing selective oxidation catalyst, involves (a) using water solution containing nitrogen element to dip the carbon-containing material, drying in the inert gas for the first roasting to obtain nitrogen-doped carbon carrier; (b) mixing the nitrogen-doped carbon carrier with the active metal component compound solution to obtain a first mixture; (c) performing the first drying and the first reduction to the first mixture. USE - Method for preparing selective oxidation catalyst. ADVANTAGE - The method is cost-effective. The selective oxidation catalyst is capable of high selectively catalyzing to obtain 2, 5-dimethyl acyl furan. The reaction solvent used is cheap and easy to obtain, avoids using organic oxidant such as nitrate, simplifies the post-processing step of the product, avoids the acid-containing waste water discharge problem, reduces energy consumption, green and environment-friendly. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for: 1. a selective oxidation catalyst, which is prepared by the method for preparing the selective oxidation catalyst, where the nitrogen-doped carbon carrier has a characteristic peak between the 399-400.5ev N1s of spectral peak XPS analysis of the nitrogen-doped carbon carrier; 2. a preparation method of 2, 5-dimethyl acyl furan, which involves (a) dissolving the 5-hydroxymethyl furfural in the organic solvent to obtain the mixed solution; (b) adding selective oxidation catalyst in the mixed solution, carrying out oxidation reaction.