• 专利标题:   Preparation and dispersion of graphene using supercritical fluid, involves pre-processing graphite raw material, mixing with dispersant and polymer, transferring to internal mixer, mixing, pumping supercritical fluid, and infiltrating.
  • 专利号:   CN107226467-A, CN107226467-B
  • 发明人:   CHEN Q, ZENG J, CHEN B
  • 专利权人:   CHENGDU NEW KELI CHEM SCI CO LTD
  • 国际专利分类:   C01B032/19, C08K003/04, C08K007/00, C08K007/24, C08L023/06, C08L039/06, C08L067/02, C08L067/04
  • 专利详细信息:   CN107226467-A 03 Oct 2017 C01B-032/19 201781 Pages: 8 Chinese
  • 申请详细信息:   CN107226467-A CN10461783 19 Jun 2017
  • 优先权号:   CN10461783

▎ 摘  要

NOVELTY - The preparation and dispersion method of graphene involves pre-processing graphite raw material to obtain expanded graphite, mixing with dispersant and polymer to obtain mixture, transferring the mixture to an internal mixer, mixing, pumping supercritical fluid into the mixer, infiltrating the expanded graphite layer by supercritical fluid, polymer shearing the expanded graphite in the mixer, stretching, dispersing, stripping the expanded graphite into graphene, dispersing the mixture in the polymer, releasing the pressure to normal pressure, and uniformly dispersing. USE - Preparation and dispersion method of graphene using supercritical fluid. ADVANTAGE - The method enables preparation and dispersion of graphene with excellent dispersibility. DETAILED DESCRIPTION - The preparation and dispersion method of graphene involves (A) pre-processing graphite raw material to obtain expanded graphite, (B) uniformly mixing expanded graphite, dispersant and polymer to obtain mixture, transferring the mixture to an internal mixer, mixing for 10-15 minutes, pumping supercritical fluid into the mixer, infiltrating the expanded graphite layer by supercritical fluid, polymer shearing the expanded graphite in the mixer, stretching, dispersing, rapidly stripping the expanded graphite into graphene under supercritical fluid permeation, and uniformly dispersing the mixture in the polymer, and (C) slowly releasing the pressure to the normal pressure after internal mixing is completed, and uniformly dispersing.