• 专利标题:   Preparation of carbon-coated graphene-nickel sulfide electrode material for supercapacitor, involves dissolving e.g. graphene oxide, nickel chloride and thiourea in solution of water and ethanol, adding aqueous ammonia and reacting.
  • 专利号:   CN104240971-A, CN104240971-B
  • 发明人:   SHEN X, JI Z, MA L
  • 专利权人:   UNIV JIANGSU
  • 国际专利分类:   H01G011/86
  • 专利详细信息:   CN104240971-A 24 Dec 2014 H01G-011/86 201513 Pages: 9 Chinese
  • 申请详细信息:   CN104240971-A CN10459256 11 Sep 2014
  • 优先权号:   CN10459256

▎ 摘  要

NOVELTY - Preparation of carbon-coated graphene-nickel sulfide electrode material involves ultrasonically dissolving graphene oxide, glucose, nickel chloride and thiourea in mixed solution of water and ethanol, obtaining mixed solution containing 0.5-1 g/L graphene oxide, 9-10 g/L glucose, 10-30 g/L nickel chloride and 5-20 g/L thiourea, adding 1.5 mol/L aqueous ammonia solution, mixing uniformly, reacting the resultant solution at 180 degrees C for 6-12 hours in a reactor, cooling the resultant reaction mixture, centrifuging, washing with deionized water and ethanol and drying. USE - Preparation of carbon-coated graphene-nickel sulfide electrode material used for supercapacitor. ADVANTAGE - The method provides carbon-coated graphene-nickel sulfide electrode material having excellent electroconductivity and capacitive property, and high specific surface area.