• 专利标题:   Synthesizing graphene oxide by oxidizing graphite powder using concentrated sulfuric acid and potassium permanganate, conducting low-power ultrasonic-assisted stripping reaction, adding hydrogen peroxide solution, and washing product.
  • 专利号:   CN104876219-A, CN104876219-B
  • 发明人:   TAN W, WU A, ZHOU C, ZHAO C, ZHOU W, SU Z, ZHOU T
  • 专利权人:   UNIV HUNAN AGRIC
  • 国际专利分类:   C01B031/04, C01B032/198
  • 专利详细信息:   CN104876219-A 02 Sep 2015 C01B-031/04 201571 Pages: 6 Chinese
  • 申请详细信息:   CN104876219-A CN10343691 19 Jun 2015
  • 优先权号:   CN10343691

▎ 摘  要

NOVELTY - The method involves: oxidizing by Hummers method graphite powder using concentrated sulfuric acid and potassium permanganate at 10-30 degrees C, carrying out low-power ultrasonic-assisted stripping reaction using a power of 80-300W, adding hydrogen peroxide solution to oxidized graphite mixed solution until product becomes bright yellow color, washing obtained product with 1 mole/l hydrochloric acid solution 3 times, washing with deionized water until neutral, and finally dialyzing resulting product to give graphene oxide solution. USE - The method is used for synthesizing graphene oxide at normal temperature (claimed). ADVANTAGE - The method enables simple, rapid and economical synthesis of graphene oxide at normal temperature.