• 专利标题:   Preparing nitrogen doped-graphene involves reacting organic material with amino and functional group e.g. amide group with graphite in reaction medium e.g. polyphosphoric acid and heat treating the prepared organic material-grafted graphene.
  • 专利号:   US2012149897-A1, KR2012064980-A, KR1216052-B1, US8575335-B2
  • 发明人:   JEON I Y, BAEK J H, BAEK J B
  • 专利权人:   JEON I Y, BAEK J H, UNIST ACADIND RES CORP, UNIST ACADIND RES CORP
  • 国际专利分类:   C07D471/22, C01B031/02, H01B001/04, H01M004/96
  • 专利详细信息:   US2012149897-A1 14 Jun 2012 C07D-471/22 201241 Pages: 14 English
  • 申请详细信息:   US2012149897-A1 US077777 31 Mar 2011
  • 优先权号:   KR126262

▎ 摘  要

NOVELTY - Preparing (M1) nitrogen doped-graphene involves: reacting organic material having at least one amino group and at least one functional group selected from carboxylic acid group, amide group, sulfonic acid group, carbonylchloride group and carbonylbromide group with graphite in reaction medium containing polyphosphoric acid and phosphorus pentoxide-, thus graphite being exfoliated with the functional group of the organic material grafted to the graphite to prepare organic material-grafted graphene; and heat treating the prepared organic material-grafted graphene at 300-1200 degrees C. USE - For preparing nitrogen doped-graphene (claimed) in industry. ADVANTAGE - The method is more inexpensive and simpler method and prepares nitrogen-doped graphene with higher purity and higher yield. The nitrogen-doped graphene prepared by the method has very excellent physical and electric properties, and particularly has superior oxygen reduction capability, compared with the platinum catalyst used at cathode of H2/O2 fuel cell so that it will replace the platinum to lower more the cost of H2/O2 fuel cell or to increase its life and further to provide a new turning point for the commercialization of H2/O2 fuel cell. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a nitrogen-doped graphene prepared by the method (M1).