• 专利标题:   Preparing graphene powder comprises e.g. reducing and preprocessing the crystalline flake graphite, then adding lithium and liquid ammonia to pretreated crystalline flake graphite, volatilizing liquid ammonia and adding water or dilute acid.
  • 专利号:   CN107934946-A
  • 发明人:   ZHANG J, YANG L, SUN Y, ZHAO F
  • 专利权人:   UNIV PEKING, BEIJING GRAPHENE INST
  • 国际专利分类:   C01B032/19
  • 专利详细信息:   CN107934946-A 20 Apr 2018 C01B-032/19 201831 Pages: 14 Chinese
  • 申请详细信息:   CN107934946-A CN11328062 13 Dec 2017
  • 优先权号:   CN11328062

▎ 摘  要

NOVELTY - Preparing graphene powder comprises (i) reducing and preprocessing the crystalline flake graphite, (ii) adding lithium and liquid ammonia to pretreated crystalline flake graphite, and (iii) volatilizing the liquid ammonia, then adding water or dilute acid and performing ultrasonic treatment to obtain final product. USE - The method is useful for preparing graphene powder (claimed). ADVANTAGE - The method: has high yield; and increases proportional efficiency of graphene compared to un-pretreated graphite. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for graphene powder obtained by above method.