• 专利标题:   Preparing graphene film used as proton exchange membrane, comprises e.g. placing graphene sample of porous substrate into Faraday cage, pumping air pressure in cavity, introducing nitrogen-containing gas, and processing by plasma processor.
  • 专利号:   CN113184833-A, CN113184833-B
  • 发明人:   WANG L, ZENG Z, ZHANG S, SONG R, HAN X, ZHU Z, CHEN X
  • 专利权人:   UNIV PEKING
  • 国际专利分类:   C01B032/184, H01M008/1016
  • 专利详细信息:   CN113184833-A 30 Jul 2021 C01B-032/184 202171 Pages: 9 Chinese
  • 申请详细信息:   CN113184833-A CN10308069 23 Mar 2021
  • 优先权号:   CN10308069

▎ 摘  要

NOVELTY - Preparing graphene film comprises placing graphene sample of porous substrate into Faraday cage, placing into plasma vacuum cavity, pumping air pressure in cavity to less than 0.1 Pa, introducing nitrogen-containing gas source under gas flow rate of 10-200 sccm, controlling air pressure at 5-50 Pa through mass flow meter, starting plasma processor, controlling starting power at 1-20 W, and processing at 15-30 degrees C for 30-120 seconds. USE - The method is useful for preparing graphene film, which is used as proton exchange membrane. ADVANTAGE - The method is simple and low in cost, and suitable for scale-up production. Compared with the traditional high-polymer-weight film, the proton flux is higher than 2-3 orders of magnitude, and the selectivity of proton/methanol is higher than 1-2 orders of magnitude. DESCRIPTION OF DRAWING(S) - The drawing shows a flowchart illustrating the method for preparing graphene film used as proton exchange membrane (Drawing includes non-English language text).