• 专利标题:   Preparation of graphene by adding natural flake graphite powder to organic solvent dissolved with alkali metal compound, performing ultrasonic dispersion treatment, filtering, cleaning, and drying in vacuum.
  • 专利号:   CN102557023-A
  • 发明人:   CHEN Y, CHU H, GENG S, SUN Z, YANG J
  • 专利权人:   DALIAN LICHANG NEW MATERIAL CO LTD
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102557023-A 11 Jul 2012 C01B-031/04 201322 Pages: 6 Chinese
  • 申请详细信息:   CN102557023-A CN10062534 12 Mar 2012
  • 优先权号:   CN10062534

▎ 摘  要

NOVELTY - Preparation of graphene using graphite micropowder as raw material by ultrasonic stripping comprises adding natural flake graphite powder with certain granularity and purity of 99-100% to an organic solvent dissolved with alkali metal compound; performing ultrasonic dispersion treatment at 20-100 degrees C for 8-50 hours, where ultrasonic frequency is not less than 10 kHz; filtering or centrifuging; cleaning; and drying the mixture in vacuum to obtain mixed product comprising n atom layers of graphene, where n is 1-5. USE - Preparation of graphene (claimed). ADVANTAGE - Compared with the prior art, the method has simple operation, high stripping efficiency, fewer graphene defects, and no wastewater; and is easy for industrial production.