• 专利标题:   Preparation of heat-resistant polyaniline conductive film involves adding heat resistant polymer to activated graphene dispersion, stirring, adding heat-resistant stabilizer, stirring and spin coating.
  • 专利号:   CN108424539-A
  • 发明人:   YANG Y, ZHANG Y
  • 专利权人:   TAICANG MEIKESI MACHINERY EQUIP CO LTD
  • 国际专利分类:   C08J005/18, C08L079/02, C08K009/04, C08K009/02, C08K003/04, C08K005/523, C08G073/02
  • 专利详细信息:   CN108424539-A 21 Aug 2018 C08J-005/18 201871 Pages: 5 Chinese
  • 申请详细信息:   CN108424539-A CN10377796 25 Apr 2018
  • 优先权号:   CN10377796

▎ 摘  要

NOVELTY - Preparation of heat-resistant polyaniline conductive film involves adding ammonium persulfate to deionized water having weight of 20-30 times, stirring uniformly, preparing an aqueous solution of ammonium persulfate, adding phosphorus trichloride and glyceryl tristearate, stirring at 50-55 degrees C for 10-20 minutes, adding aniline, stirring, subjecting to a reaction vessel, introducing nitrogen gas to adjust the temperature of the reaction vessel to 65-70 degrees C, adding obtained aqueous ammonium persulfate solution, stirring for 4-5 hours, discharging the product, obtaining phosphorus-doped polymer emulsion, adding bisphenol A to phosphorus-doped polymer emulsion, stirring uniformly, increasing the temperature to 90-95 degrees C, stirring for 1-2 hours, suction-filtering, washing filter cake, drying at room temperature, obtaining heat resistant polymer, adding obtained polymer to activated graphene dispersion, stirring, adding heat-resistant stabilizer, stirring for 3-4 hours and spin coating. USE - Preparation of heat-resistant polyaniline conductive film. ADVANTAGE - The method efficiently provides heat-resistant polyaniline conductive film having high stability, mechanical strength and heat stability.