• 专利标题:   Preparing cobalt nickel-graphene composite wave absorbing material comprises e.g. taking cobaltous nitrate hexahydrate as raw materials, placing cobalt/nickel-graphene oxide composite material in tube furnace, and heating.
  • 专利号:   CN111615320-A
  • 发明人:   LIN Y
  • 专利权人:   FUJIAN MEIQING HEAT TRANSFER TECHNOLOGY CO LTD
  • 国际专利分类:   C01B032/194, H01Q017/00, H05K009/00
  • 专利详细信息:   CN111615320-A 01 Sep 2020 H05K-009/00 202080 Pages: 6 Chinese
  • 申请详细信息:   CN111615320-A CN10622038 30 Jun 2020
  • 优先权号:   CN10622038

▎ 摘  要

NOVELTY - Preparing cobalt nickel-graphene composite wave absorbing material comprises (i) taking cobaltous nitrate hexahydrate, nickel(II) nitrate hexahydrate and tetrasodium ethylenediaminetetraacetate as raw materials to obtain cobalt/nickel precursor by hydrothermal method, (ii) dissolving graphene and cobalt/nickel precursor in ultrapure water, ultrasonically dispersing for 2 hours to obtain suspension, adding hydrazine hydrate, and transferring into the autoclave, placing in a vacuum drying oven, heating at 200 degrees C for 24 hours, and cooling to room temperature, washing repeatedly with deionized water and ethanol to neutrality, and drying at 60 degrees C to obtain cobalt/nickel-graphene oxide composite material, and (iii) placing cobalt/nickel-graphene oxide composite material in tube furnace under nitrogen atmosphere, and heating at 700 degrees C for 5-6 hours to obtain final product. USE - The method is useful for preparing cobalt nickel-graphene composite wave absorbing material. ADVANTAGE - The composite wave absorbing material has frequency band width of 12.2 GHz, maximum reflection loss of up to 46.3 dB (13.8 GHz), and low density. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for cobalt-nickel-graphene composite absorbing material obtained by above method.